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Edible films and coatings are a thin layer of material that used on the surface and between different layers of nutrients. Biopolymers such as polysaccharides, proteins, lipids and their mixtures are used for the preparation of the edible films and coatings. Due to consumers demand for access to high quality materials and their concern because of the problems caused by the use of artificial preservatives, as well as environmental concerns arising from the accumulation of synthetic polymers, the idea of using biodegradable biopolymers as a replacement for the plastic packaging was strong. Efficiency and functional properties of edible films and coatings is dependent on intrinsic properties of ingredients of films, namely, biopolymers, plasticizer and other additives. The useful properties of edible films and coatings are capability of eating and biodegradation of them. Some properties of edible film sand coatings, such as preventing moisture transport and volatiles out of food, selective throughput oxygen and carbon dioxide, delaying surface dehydration, tissue changes, barrier against fat sand oils transports, increase nutritional value, preventing dripping, microbial growth and rancidity, Maintaining the quality of Aquatic and their products against physical damage caused by their transportation, increase the shelf life of them. For industrial use, more scientific studies are needed to determine the mechanisms of the film formation from biopolymers for optimizing their properties. Biodegradable compounds used in this study for aquatic coating and their effects on maintaining the quality of fish and their action mechanism has been investigated.

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  Nowadays, edible films are commonly and increasingly used for covering food products, as a replacement for synthetic films. Their advantages are being edible, safe and functionally effective. Many researches have been being done in this regard. This article reviews fundamental and applied aspects of edible films in food industry including definitions, classifications, applications and common types of used materials.

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Being biodegradable, edible and efficient have caused edible films to be widely investigated and used as a good replacement for synthetic materials in packaging of food products. Coating confectionaries, fresh fruits and vegetables, some meat products, some dairy products, chocolate, snacks, breakfast cereals, fish and poultries, frozen products, dried and freeze dried products are from those food materials that are regularly coated by edible films. The efficiency of edible films depends on their quality parameters, the latter are principally affected by the type of film-producing materials as well as its method of preparation. This article reviews quality parameters of edible films, their test methods and principal production techniques.

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Aims: In this study, gelatin was extracted from Siberian sturgeon waste and used in film making.
Materials and Methods: Gelatin was extracted using NaOH and HCl. After evaluating the extracted gelatin properties (bloom grade, pH, zeta test, melting and setting temperature and time), the edible film was prepared by using glycerol.
Findings: The results showed that the extraction efficiency of the gelatin was %20.06. The protein content, pH, degree of gel hardness, setting and melting temperature and time were 79.2 ± 0.6%, 4, 160.2 ± 0.4 g, 13.1 ± 0.2 ° C in 180.3 ± 0.5 seconds and 19.33 ± 0.5 ° C in 140.66 ± 0.5 seconds, respectively. Zeta potential indicated a positive surface charge in gelatin. The thickness, moisture, solubility, tensile strength, tensile strength and permeability tensile strengths properties of gelatin film reported 0.05 mm, %10.2 ± 1.5, %79 ± 3.7, 30.01 ± 0.7 MPa, %77.5 ± 3.6 and 3.5 ± 0 g mm/h mm²kpa×10^-6­, respectively. SEM images of the film showed smooth structure without cracking. Moreover, the FTIR result showed the formation of amide bands in the region of 3277.62, 1633.92, 1530.11 and 1236.49 cm^-1.
Conclusion: Due to the efficiency and properties of gelatin, and the mechanical and physical properties of the edible film, it can be used as a good candidate for the production of biodegradable films in food storage.

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This work was aimed to investigate the potential preparation of an biodegradable film preparation from bitter vetch seed protein and determine some of its physicochemical properties. The film was cast from bitter vetch protein concentrate (BPC) (5 g/ 100 ml alkaline water) and glycerol (50% w/w of BPC). The moisture content (MC), color, tensile strength (TS), elongation to break (EB), water vapor permeability (WVP) and surface hydrophobicity of the film were measured. The film with MC of 27.69%, TS 5.04 MPa and WVP 0.72 (gmm/KPa.h.m² ) ws comparable with other protein films but its red and yellow indices in color (a=22.41 and b=37.20) and EB were higher than other protein based-films. Its surface hydrophobicity (49.83^°) was higher than that of soy and sodium caseinate protein films and lower than red bean protein film. In general, according to the results, it seems that the film obtained from BPC has a good potential to be used in packaging applications.    

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In recent years, Mg alloys have received much attention as a promising candidate for raw material in biodegradable vascular stent. Forming of Mg alloys is difficult because of poor workability of them at room temperature. Hence this presents a technological barrier to the fabrication of initial micro-tube for a biodegradable stent. With regard to high biodegradability of the magnesium alloy WE43 to manufacture biodegradable stent, it has been selected as initial with casted structure. In this study, for enhancing mechanical properties and attaining micro tube a combination of equal channel angular pressing (ECAP) with extrusion and micro extrusion was used and Mg bars were fabricated to high-quality micro-tubes with refined microstructure. Fine-grained size billets of the WE43 alloy were obtained by one-pass of ECAP. The processed Mg bar was extruded into a bar with 5 mm in diameter. Finally, a UFG and high strength micro tubes with an outside diameter of 3.4mm and a wall thickness of 0.25mm were successfully produced by micro extrusion process. Mentioned processes were simulated using finite element (FE) simulations. The result shows the grain size of Mg incredibly reduced after this combined method and mechanical properties were significantly improved.

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Objective: Dendrimers are three-dimensional nanostructures that have numerous applications in medicine, including drug delivery and imaging. Although anionic dendrimer polyethylene glycol–citrate has a high potential to increase solubility of water-insoluble drugs and drug delivery, its multi-step synthesis procedure is time consuming. In addition, toxic substances such as dichloromethane are used in its synthesis procedure. In this study, we have developed a simple one-step synthesis method using green chemistry. Methods: We examined four different methods to improve the synthesis method of this dendrimer. Products were characterized by FTIR, LC-MS and DLS. Cytotoxicity was assessed by the XTT method. Results: We synthesized a G2 polyethylene glycol–citrate dendrimer in one-step without purifying G1. This process was chosen as a beneficial method for synthesis of the G2 dendrimer. When compared with previous methods, this procedure had higher efficiency and greatly reduced response. This procedure used nontoxic materials. XTT assay results showed that this dendrimer created by green chemistry had no cytotoxicity in Hela and Vero cells up to a concentration of 800 µM. Conclusion: One-step synthesis of anionic polyethylene glycol-citrate G2 dendrimer is a simple, beneficial production method. The dendrimer is biocompatible and can be used as a suitable carrier for drug delivery purposes.

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Nowadays, the use of biodegradable packaging based on natural ingredients has attracted much interest from researchers. In this research different concentrations of persian gum (PG) (0, 0.25, 0.5, 0.75 and 1%) with different concentrations of carboxymethyl cellulose (CMC) (1 and 1.5%) were used to optimize biodegradable film production. For optimization of film production, maximum transparency value, contact angle, tensile strength, strain at break and minimum solubility, swelling and water vapor permeability were calculated. The results of the model showed that the effect of carboxymethyl cellulose and persian gum on all responses were significant (P <0.05) and increasing the percentage of carboxymethyl cellulose and persian gum increased solubility, swelling, tensile strength and contact angle and decreased moisture content, water vapor permeability permeability and transparency value. Based on the results of model prediction and comparison with experimental values, carboxymethyl cellulose at 1.5% and persian gum at 0.65% is the best result.
 

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In this study, the effect of various treatments with cellulose nanocrystals (NCC) and ZnO during papermaking and coating with these nanomaterials and polycaprolactone (PCL) on the barrier properties of the papers was investigated. The samples were studied by Field Emission Scanning Electron Microscope (FESEM) and X-ray diffraction (XRD) devices. In this research, the nanomaterials and the polymer with the specified condition (4%, 6% NCC, 3% ZnO and 10% PCL) were added to the paper pulps during the papermaking and also as a coating agent. Cationic polyacrylamide used as a nanomaterials retention aid in the papermaking process. the results showed the barrier properties (water absorption, air permeability and grease absorption) of the treated papers were improved but the effect of NCC% increment was more clear in the enhancement of the barrier properties and the treated papers with the nanomaterials mixture had the best barrier properties.furthermore the barrier properties of the coated papers were enhanced with the nanomaterials addition and the NCC nanoparticles had the main role, also the mixture of nanomaterials and PCL had the best barrier properties. Also, the barrier properties of the coated papers were higher than the treated papers.
 

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Recently, the design and production of biodegradable films have received special attention than synthetic packaging due to the reduction of environmental pollution. The aim of this study was to investigate the effect of Persian gums (1%) and gellan gum (1%) on the physical, mechanical and morphological properties of composite films based on sodium caseinate (10%) as film reinforcing agents. The films were synthesized by solvent evaporation and the effect of each gum on the characteristics of the composite films was evaluated. The results showed that the addition of gums strengthened the composite films. So that the composite films showed mechanical resistance and good barrier properties versus moisture and light. The surface properties and morphology of the films also showed that the gums were well computability to the casein film and formed uniform and stiff films. In addition, composite films had acceptable transparency. Thus, it can be concluded that the use of composite films and the combination of different polysaccharides with protein matrices can improve the properties of the resulting films. On the other hand, by adding antimicrobial and antioxidant agents to biodegradable films, they can be considered as active packaging.

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The aim of this research was to investigate the feasibility of composite and laminated chitosan (CH) and whey protein isolate (WPI) film preparation which was containing cumin essential oil and chitosan nanofiber. Production of composite film was possible by decreasing WPI pH to below its isoelectric pH. Double-layer was also prepared by pouring WPI solution on dried CH film. amount of active agent and nanofiller was fixed (125 mg/100ml) and only the effect of CH/WPI ration and film type (laminated or composite) on the properties of films was arudied by RSM analytical method. The color, watercontact angle, moisture absorption, solubility, water vapor permeability and mechanical properties of films were determined. By using desirability function and according to the results, optimum formulation of composite film (65.14% WPI and 34.85% CH) and laminated film (49.01% WPI and 50.99% CH) was achieved. Microstructure of optimized films was analyzed by FTIR, FE-SEM and XRD tests. Results of FE-SEM indicated a heterogenous stracture in composite film but without any phase separation. Also, at the laminatred film good attachment between two layers of CH and WPI was observed. Semi-crystalline stracture of composite film was approved by XRD analysis and there was no detectable difference between peak intensity and crystalline stracture of composite and laminated film. there was a slight difference in the FTIR spectra of composite and laminated films. According to the results, the characteristics of composite film in comparison to laminated film had better accordance with the used prediction model. But the laminated film exhibited better morphological characteristics and could be suggested for preservation of different foods due to its high potential for use in food packaging.

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Edible films, which in addition to creating beneficial effects by carrying antimicrobial compounds, antioxidants, etc., have biodegradable properties, have attracted the attention of many researchers. In this study, the gum obtained from the inner pod of bean with two concentrations of glycerol (40 and 60%) and three concentration of oregano essential (1, 2 and 3%) oil was used to produce biofilms. After studying the physicochemical and mechanical properties of the resulting films, the best treatment was combined with titanium oxide nanoparticles in two concentrations of 1 and 2% and its antimicrobial properties were also investigated. The results showed that increasing the essential oil raised the film thickness, while high concentrations of essential oil decreased the moisture content of the films. Although the addition of essential oil reduced the solubility of films compared with control sample, but in the treatments with essential oil, increasing the essential oil reduced the solubility of the film. Increasing the concentration of essential oil also increased turbidity and free radical DPPH activity. High concentrations of essential oil decreased the lightness of the films but increased the yellowing and redness compared to the control sample. Due to the interaction of the oil in the essential oil with the gum, the cohesion of the polymer network decreased and consequently, the tensile strength and the elongation factor at the break point decreased. Antimicrobial effect of films with 3% essential oil and 2% titanium oxide had the highest inhibitory area in the disk diffusion test with other samples on Staphylococcus Aureus, Escherichia coli, Salmonella Typhoid, Bacillus Cereus and pseudomonas Aeruginosa significantly (p<0.05)

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In this study, different concentrations of aqueous extract of Chubak root (at levels of zero, 0.5, 1, 1.5, and 2%) with different concentrations of rosemary essential oil nanoemulsion (zero, 0.5, 1, 1.5, and 2%) was used to optimize the production of biodegradable gelatin-based film. Test responses were statistically significant for all fitted regression models at 99% confidence level. To optimize film production, maximum transparency, contact angle, tensile strength, Elongation at Brake to the point of rupture and minimum solubility, swelling and vapor permeability were evaluating. After fitting the models, the results showed that the effect of aqueous extract of Chubak root and rosemary essential oil nanoemulsion on all responses was significant (P <0.05). Increasing the aqueous extract of Chubak root and nanoemulsion of rosemary essential oil increased the thickness, contact angle and Elongation at Brake to the point of rupture and decreased moisture content, vapor permeability, transparency, solubility, tensile strength and swelling. Based on the results of model prediction and comparison with experimental values, aqueous extract of Chubak root at a concentration of 2% and nanoemulsion of rosemary essential oil with a concentration of 0.77% were obtained as optimal values.

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Biodegradability of food packaging materials is one of the most important parameters of modern food packaging industries. Jug cheese is a hard, somewhat acidic and salty cheese that has a dry appearance and has a higher nutritional value than salt water cheese due to the preservation of nutrients in the curd. Therefore, the aim of the present study was to use a biodegradable film of polyvinyl alcohol and pinto bean starch containing cinnamon, garlic and ginger essential oils to improve the physicochemical and sensory properties of jug cheese and compare with conventional packaging. For this purpose, jug cheese in biodegradable biodegradable film based on polyvinyl alcohol / pinto bean starch (80/20 %) containing different concentrations (3.125, 6.25 and 12.5%) of essential oils Cinnamon, garlic and ginger were packaged and their physicochemical and sensory properties were evaluated during 60 days of storage at 4 ° C and compared with the control sample. The results showed that the use of essential oils and increasing their concentration in biodegradable film caused a significant increase in moisture content and a significant decrease in weight loss and dry matter in jug cheese samples during storage. Also, with increasing storage time, pH, humidity and weight loss decreased significantly (P<0.05) and the amount of acidity, salt and dry matter increased significantly (p<0.05). The sensory evaluation score of the jug cheese samples packed in biodegradable film containing 3.125% of cinnamon and ginger essential oil after 60 days of storage was higher than the control sample. The use of biodegradable films based on pinto bean starch and polyvinyl alcohol along with cinnamon and ginger essential oils are solutions that can improve the physicochemical and sensory properties of jug cheese during storage and Also prevent environmental damage.

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In this study, biodegradable packaging based on gelatin biopolymer (at a concentration of 3% w/w) containing nanoparticles of titanium dioxide (at a concentration of 1% w/w) and saffron extract (at a concentration of 2% v) by evaporation method was synthesized. In this study, physical properties (thickness, transparency, moisture content, solubility and water vapor permeability), mechanical, antimicrobial and antioxidant properties, structural and transparency properties of films were investigated. After analyzing the data, the results showed that the effect of saffron extract and titanium dioxide nanoparticles on all the studied properties was significant (P <0.05). Addition of titanium dioxide nanoparticles and saffron extract increased the thickness, improved the mechanical properties and reduced the moisture content, water vapor permeability, transparency, and solubility. Also, nanocomposite films containing titanium dioxide nanoparticles and saffron extract showed antioxidant properties (% 80%) and acceptable antimicrobial effects, especially against gram-positive Staphylococcus aureus bacteria. According to the results of this study, this type of packaging can be suggested as a suitable alternative to synthetic packaging.

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Due to the fact that the use of biodegradable films helps to protect the environment, in this study, the physical, mechanical, antioxidant and thermal properties of polylactic acid films containing polypyrrole, ‌ polyaniline and copper oxide were investigated. The results showed that due to the addition of oxidant nanoparticles, the thickness of the films increased and their water vapor permeability decreased significantly. The solubility of the films also decreased significantly with increasing the amount of copper oxide nanoparticles. The resulting films showed less flexibility due to the addition of polyaniline and polypyrrole, while their resistance to failure showed a relative increase. Antioxidant activity of polylactic acid films containing polypyrrole / CuO and polyaniline / CuO showed a significant increase compared to pure polylactic acid (p<0.05). Pure polylactic acid film did not show any electrical conductivity, If the addition of polypyrrole and polyaniline increased the electrical conductivity of the films, the copper oxide nanoparticles also had no significant effect on the electrical conductivity. These films can be used as biosensors in food packaging due to their conductivity and suitable thermal, mechanical and water vapor permeability properties.

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The aim of this study was to produce a new bioactive composite film using whey protein concentrate and jujube mucilage reinforced with postbiotics of Bacillus coagulans IBRC-M 10807. For this purpose, four films including whey protein concentrate film (WPC), whey protein concentrate film containing B. coagulans postbiotics (WPC+PBs), whey protein concentrate film and jujube mucilage (WPC+MUC), and whey protein concentrate film and jujube mucilage containing B. coagulans postbiotics (WPC+PBs+MUC) each in three replicates of production and their physicochemical, antimicrobial, antioxidant and mechanical, were compared in the form of a completely random design and with the analysis of variance method. The results showed that the addition of postbiotics and jujube mucilage caused a significant increase in the moisture and solubility of the films (P<0.05). Adding postbiotics causes an inhibitory effect against Staphylococcus aureus and Escherichia coli bacteria (P<0.05). The addition of postbiotics and jujube mucilage caused a significant decrease in the L index of the produced film samples (P<0.05). The results showed that the a and b indexes increased significantly with the addition of postbiotics and jujube mucilage (P<0.05). The results of the present study showed that the produced bioactive biocomposite film has the potential to be used in food packaging.
 

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In this research, flax seed mucilage was extracted. Composite film of sodium alginate and flax seed mucilage was prepared. Norbixin pigment and tungsten oxide (WO3) nanoparticles were used to modify the film structure. The color, crystallite, thermal and mechanical properties of the films were investigated. Also, the antibacterial properties of the prepared films against Escherichia coli and Staphylococcus aureus bacteria were investigated. The obtained results showed that the pure alginate/mucilage film does not have very high transparency, which is reduced by adding tungsten oxide nanoparticles and norbixin pigment. The effect of tungsten oxide nanoparticles in reducing film transparency has been greater than that of Norbixin. Examining the factor a (green-red) shows that this factor has increased with the increase of Norbixin and tungsten oxide nanoparticles. Examining factor b (blue-yellow) shows that with the increase of Norbixin and tungsten oxide nanoparticles, this factor has increased. By examining the XRD spectrum of the pure alginate/mucilage film, it was found that this film showed two broad peaks at 2θ of 10° and 20°, which indicates the relatively amorphous structure of this film. In the alginate/mucilage film modified with tungsten oxide nanoparticles, the peaks related to the crystalline nanoparticles in 2θ of approximately 25, 30, 35, 40, 50, 55 and 65 degrees are quite clear, which shows that these nanoparticles improve the crystalline structure of the film. By examining the TGA curves of the films, it was found that the addition of tungsten oxide nanoparticles and norbixin pigment increased the thermal stability of the film. Examining the antibacterial property of the films showed that the addition of tungsten oxide nanoparticles and norbixin pigment increased the antibacterial property of the film significantly (p<0.05).